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Analysis using X-rays
Energy Dispersive X-ray fluorescence spectrometer (EDX) is the instrument
to perform qualitative and quantitative element analysis in the
range from 6C/11Na to 92U and is the ideal tools for non-destructive
applications. EDX is used in many different applications areas
in the chemical, electronic and food industries as well as refineries.
It can be used with solid, powder and liquid samples. This is
achieved by applying X-ray to the sample and then analysing the
re-emitted element characteristic fluorescent X-ray. Security
functions effectively prevent exposure to X-rays at all times.
Easy handling and improved detection limits
With a simple push of a button, elements ranging from sodium to
uranium can be analysed quickly and easily. In addition, the
software enables measuring conditions to be adapted to the sample
characteristic. For precise analysis of lighter elements the
systems can be operated optionally under vacuum or under a helium
atmosphere. The built-in five-filter assembly (zirconium, aluminium,
titanium, nickel and molybdenum) effectively reduces interferences
and increases the signal quality. This way, the limits are markedly
improved for detection of e.g. lead, cadmium, chlorine or chromium.
High flexibility
The large sample chamber accepts samples up to 300 mm diameter
and 150 mm height. Additionally, many accessories are available,
for instance a precision stage for accurate sample positioning
as well as various sample turrets for 8 or 16 samples. The detector
system requires liquid Nitrogen (N2) but a thermoelectric cooled
detector system is also available. For the measurement of small
samples, the X-ray is decreased easily using optional collimator
assemblies. Two different assemblies are available:
- 1, 3, 5, 10 mm
- 0.3, 1, 3, 10 mm.
The exact positioning of small samples can be monitored accurately
using an optional colour CCD camera.
WEEE and RoHS
In addition, the EDX series offers, with respect to WEEE (Waste
Electrical and Electronic Equipment) and RoHS (Restriction of
the use of certain Hazardous Substances in electrical and electronic
equipment) simple and fast decision-making criteria in order
to adhere to these directives. The EDX systems enable analyses
of mercury, cadmium and lead in polymer building parts (such
as casings and cable insulations) down to the ppm range. During
EDX analysis, hexavalent chromium, PBB (polybrominated biphenyls)
and PBDE (polybrominated diphenyl ether) are detected as elemental
chromium and elemental bromine.
>> Read about Shimadzu's RoHS compliance and commitment to sustainable
development and the environment. |